Techniques
Energy Dispersive X-ray Analysis

Energy Dispersive X-ray Analysis (EDX) is employed in Scanning Electron Microscopy (SEM) and Transmission Electron Microscopy (TEM) for local elemental identification. The incident electron beam induces X-ray fluorescence in the sample which is energy-analysed using a cooled semiconductor detector. The element-specific spectral lines are then identified to give the local elemental composition.

EDX provides a powerful tool for identifying local composition within TEM images and is utilised extensively in applications ranging from failure analysis to elemental mapping. We addtionally offer Electron Energy Loss Spectroscopy (EELS) which provides elemental mapping with higher sensitivity to low mass elements.

Energy Dispersive X-ray Analysis

TEM-EDX elemental analysis of individual metal catalyst particles, with an example EDX spectrum shown inset.

Key Information
  • Local elemental identification
  • Quantitative micro- and nano- analysis
  • Sensitivity down to sub-atom%
  • Elemental composition as a function of depth from cross-sectioned samples
  • Analysed area: Few nm to 3 mm (dependant on SEM/TEM instrument employed)
Common Applications
  • Elemental composition & stoichiometry
  • Compositional variations & elemental mapping
  • Particle & contaminant analysis
  • Defect / flaw analysis
  • Layer composition
  • Cross-section analysis
CEMMNT Benefits
Industry Sectors